不饱和脂肪酸检测报告(油脂)

项目报告
1 样品信息Sample description
收到油脂样品xx个,a和b
A total of xx oil samples, where received by the customer.
2 材料与方法Materials and Methods
2.1 试剂Chemicals
所有的溶剂与试剂均为色谱级,α-亚麻酸,亚油酸,油酸标准品购于xxx
All chemicals and solvent were HPLC. Standard: α-linolenic acid, linoleic acid, oleic acid and were purchased from xxx.
2.2 样品处理Sample Preparation
1) 将样品摇匀,称取0.2g左右的样品; 2) 0.2g样品加入0.5 mol/L的xxx溶液10 mL,回流提取30 min; 3) 冷却,以0.5 mol/L盐酸溶液调节至弱酸性(pH = 5),用60~90°C的xxx振摇提取3次,每次20 mL,合并xxx,室温挥干; 4) xxx加入无水乙醇2 mL,摇匀并用0.22µm滤膜过滤,进样10 µL。
2.3 HPLC分析HPLC Analysis
本实验所用的仪器为Agilent高效液相色谱仪,配备紫外检测器。
色谱柱为xxx C18 (250 mm*4.6 mm, 5 μm),流动相为xxx-0.1%xxx(80:20, v/v),流速为1.0 mL/min,柱温为30℃。
3 结果Results
色谱图Chromatogram


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